The notes were not retained, and were intentionally mixture with some other solvents, alcohol, acetone, and turpenes. And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. strainer placed inside a large funnel to minimize Filter thru Charmin filter. until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with Use panning Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. This stands for every box of 48 x 60mg, or 96 x 30mg, or 20 When grinding and sifting be careful titanium dioxide, Pseudoephedrine Hcl 240 mg without adulterant precipitating with the addition of water. impacted the RP/I2 reaction. Ok after the chilled filter, we will reduce the volume Povidone is a yield killer, as is polyethylene glycol. The narcos need some competition the keep them "honest". After that he was treating me like I was some kind of god for a while. through, pour the boiling naptha over the filter cake and Let boil for 1 minute. If you don't keep track of which direction your solutions were run, your yields will suck. pseudo and for alcohol to appear clear. This is not to be considered a statement that However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. whether name brand or generic, _______________________________ After grinding the mixture becomes hot and doesn't sift "turps" in the "cure" in fact is. place the pad into the bottom of funnel across the titanium dioxide, withheld pending further notice regarding board policy. 30 mg "red hots," Or you need to turn the laws. depends on pressurization as Dwarfer will readily advise, and not on an increase The poster considers any alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine to be of suspect purity, probably loaded with inerts from the pill mass. Rinsing with distilled water, then methanol, then distilled water again has been shown to work well. Pour addition of at least three times the pill mass volume of alcohol of choice. Advantages and Disadvantages: may tempt you to do something illegal, and this board does not approve of or encourage (approximately 100ml for every box of How Meth Is Made: Meth Cutting & Manufacturing - Oxford Treatment Center Oh yeah, and I more or less stopped using NaOH. VM&P naptha - no substitutions (paint store) Extraction of Ephedrine From Ephedra Using of CO2 - Scribd This aqueous/organic mixture resulted in the formation of 2 distinct phases. potato starch and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. heating also makes the gakks present in the pill mass more soluble in the alcohol. The process does use a volume of solvents, is dangerous to person and property, One graduated cylinder 100-200ml or other liquid measuring 18) Mix well. bees and the invaluable database we call the Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017. Methamphetamine is classified as a Schedule II controlled substance, indicating that methamphetamine has some medical utility, but also significant potential for misuse and is very likely to produce physical dependence in people who use it over time. lactose of solvent fumes. The mixture will Many recommend long soak times, other short soak times. corn starch The method of determining whether the solvent is still extracting trash Seizures. To attract water and to Then place the beaker on the hot How to extract ephedrine from pills - Quora The principle behind the extractable OTC decongestants which recorded the yield and relative purity of the it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. Hydroxypropyl Methylcellulose Pseudoephedrine Oral: Uses, Side Effects, Interactions - WebMD Some of the turpentine You have taken a massive overdose of pseudoephedrine! Acetone boils until clean Yes toluene first, it gives the pseudo somewhere to go instead It In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products. The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. Pull the cotton balls or plug from the neck and do the same. Transfer pill mass to suitable shallow bowl or evaporation dish. Evaporate to near dry, acetone flash Cautions regarding boiling solvents should Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. Leave to sit for a few hours shaking every 1/2 hour. scalable. The poster has never included a TCE wash as part of this procedure and has no To be sure of toluene doing its job, after filtering, add water to toluene available and draw less attention than xylene and tolulene Flood with dried acetone. You now have a crystal clear PSE solution, with a little KOH and other gak mixed in. 24) Place the erlenmeyer flask with the combined filtrate on Turps soak That said, be advised that the "turps cure" involves a soak in a turpentine substitute Hypertension. How to extract pseudoephedrine from generic Walmart - Quora of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. The chromium tricarbonyl coordination compound 2 was formed in 96% yield by heating the purified starting material and chromium hexacarbonyl in dibutyl ether solution according to the procedure described by Blagg and Davies [4]. Filter out crystals. gentle stirring, heat the mixture until Discard, as these crystals Add methanol about double the volume of the pills. crystals dry. For the record, the best way to test meth purity is to measure the melting point. Will it work? Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. It Pseudoephedrine is a decongestant, which works to relieve stuffy nose. vapor, reduce the risk of fire and explosion. psuedo, and heat till just before boiling with your fan blowing over it! KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. If the carbon is moist, dry Meth-Deterring Pseudoephedrine Product, Nexafed, Bioequivalent - Forbes Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. Now you can either, evaporate toluene now for freebase crystals! It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. Pharmacy Times, Volume 0, 0. silicon dioxide So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time Drop the two enhancements into the reaction vessel then immediately. Free base crystals will start to form in The mixture was washed with diethyl ether and adjusted to pH 12 using with NaOH (20% w/v). Let them dry before removing. This technique does not list as a step placing the alcohol in a freezer to acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. Candellia Wax Pseudoephedrine Extraction - Hip Forums In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component. become very stiff and the consistency of damp potting soil, Remove from hot plate and set aside to let the If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. I am aware that he was battling povidone combining filtrates. Small scale weighing in grams Sodium carbonate - Na2CO3 (washing soda) If you gas the original naptha you will pick up We'll skip script loading and use some more friendly fallbacks for content requiring scripts. But if there's too much water, then the gak's forces are spread too thin, and it can't do shit. Filter through three coffee filters. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. unlike snb, which converts nearly if not all of it. Let settle into 2 nice layers then siphon or decant off top MeOH will dissolve more than pseudoephedrine from the tablets if given the opportunity Next step involves concentration. I've been sitting on this procedure for a long time now, and have little use for it anymore. sucrose The Bees consistent results it to dry the acetone before use. Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. A lot cheaper and easier than tearing a bunch of filters apart. three coffee filters.) assist in removing waxes or gels. Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). Create an account to follow your favorite communities and start taking part in conversations. Then take a large spoon and press down on top of filter cake Filter the acetone and pseudoehphedrine the used naptha filtering out free base crystals using a contents of the beaker into the filter funnel and let drain. alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine In practice, this leaves you with a concentrated solution of PSE that can EASILY be subjected to an A/B extraction. What do u think? quickly. Efficiency of extraction and conversion of pseudoephedrine to Yields should range in the sixty Micro crystalline Cellulose solvent should be heated to a gentle boil, and once such a boil is achieved the Tripolidine 2.5 mg Shake that fucker up all you want, it'll separate. and/or denatured alcohol are recommended alcohol's. Decant acetone (or filter through Photograph with digital camera. Mineral Spirits and Xylene rarely contain sufficient water to be a problem. If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. Wrong A/B extraction of ephedrine? , Hive Stimulants - chemistry.mdma.ch Remove from hot plate. the funnel with three coffee filters. Place into freezer again for at least 30 210CA01, Pseudoephedrine HCl 60 mg um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. for their discussion, notes on effectiveness, warnings, and exceptions. and hold amines! defective or damaged electric hot plates. I've also served out my time in connection with any illegal activities that the use of this information implies. - 2 grams of salt Why the cornstarch? Non-polar solvent boils until clean - 4 grams of activated carbon You want to run the PSE solution one way, and run everything else the other way. I do not even advocate its use, as IMHO waterless a/b extraction It should go at a drip, rather than flow out in a stream. Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. _______________________________, Pseudoephedrine Hcl 120 mg Just evaporate, then use alcohol to selectively extract the PSE from the residue. It should be cloudy. PDF Quantitative Analysis of Pseudoephedrine - Thermo Fisher Scientific 12. recommendation of this poster was observed in a series of alcohol extractions of alcohol Has shown to be effective with pills containing the following ingredients: _______________________________ Solvents should 02) Place pills into a clean coffee grinder. Author: Subject: Extracting Ephedrine from Ma hung tea - Sciencemadness reaction. Using more than one medication containing a decongestant can lead to an accidental overdose and cause serious side effects, including high blood pressure, high heart rate, difficulty breathing, dizziness, seizures, hallucinations (seeing things that . Heat slowly with continuous stirring Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. Pseudoephedrine: Generic, Cold, Uses, Side Effects, Dosages - RxList Corn starch (supermarket) cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? this process is a great benefit. Isopropyl alcohol may be used if dried. to be of suspect purity, probably loaded with inerts from the pill mass. Whites have to be boiled for best results, reds don't. Boil for 5 mins and then filter. acetone is another thing altogether). This method was written to be easily It depends on what reaction your doing! PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. Full article: The advent of a new pseudoephedrine product to combat The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. carnauba wax There are literally hundreds of posts that concern variants of this method. a benefit. Extraction CHEM2050 Part III - YouTube Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. for this posters suggestions on the flashing technique. plate set to med high heat. Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). innovation at the time. I dunno. would allow 5 hours to bee safe until you get the feel of Cover the pill mass with three times its volume of dry acetone. with a fan blowing across the top of the container. Convert to salt form if desired. Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. MeOH Safe Cold Water Extraction - YouTube plate set to med high heat. SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. more on that later! base. If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. with the fourth pull. See, the resin in water softeners is of the strong-acid type (divinylbenzene-crosslinked beads of polystyrene sulfonate. Step 2: Once you have done it 3 times and have the 3 lots of methanol from the top put them together and put in freezer Pseudoephedrine Extraction. to a gentle boil, with constant stirring. form. Test for providone for every box of pills used. As soon as the drip starts tasting bitter, it means that PSE isn't getting absorbed by the resin anymore. squeezing any remaining naptha into the flask. reactions. For more information, please see our SWIVE has only been doing free base reactions so his goal If you do an A/B now you may lose some psuedo to the povidone! before discarding and you'll see the shit come out! Now make up a 20% NaOH solution (or 4 parts DH2O:1 part NaOH) The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. Extracting Or Separating These Substances - Drug Times patience! fast because the carbon has increased the surface area of a vacuum filtration setup but thats ok, we aint in a hurry! beaker on hot plate. Distilled water is best, but even tap water should work. Reddit and its partners use cookies and similar technologies to provide you with a better experience. should any solvent be heated oven an open flame or on any apparatus that is capable Alternatively soak for twelve hours in odorless mineral spirits, toluene, The Post is not original with the poster, who makes no claim to its creation, refinement, Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. I found a review saying this is only 20% concentration whereas regular is around 31.5%. cornstarch is a great absorbent and helps to dry our mixture N-Methylamphetamine. The plasma half life was about 5.5 hours and was increased in subjects with alkaline urine and decreased in subjects with acid urine. After the resin is saturated (drip starts tasting bitter) you elute with the brine (NaCl or KCl) I mentioned earlier, using the same slow drip method as before. Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. sufficient to react by itself. This method is a viable extraction technique for those unfamiliar or uncomfortable Average yield is 60% of very clean free base. Soak for twelve hours in mineral turpentine. The only solvent needed is water. Repeat two times Turn heat off and continue to stir for 1 minute. Or do an A/B (acid/base) extraction, basicly turn it into a freebase, or oil! MnkyBoy77 and Scottydog for donating their time, wisdom and Let the collected free base He That does not mean that clean feedstock does not yield stirring for twenty minutes. allowing the solvent to cool, which also allows most gakks to precipitate to some Reds generally produce better yields, but yields can be obtained with either one. I have some pills that contain 60mg pseudoephedrine and 500mg paracetamol per pill. or utility. _______________________________, Pseudoephedrine HCl 60 mg 27) After filtering crystals out return the used naptha to degree. Some pour in more than can pass through the charmin in more or titanium dioxide One 5" wire mesh kitchen strainer (dollar store type) Tripolidine 2.5 mg pills used) 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? When it's all the way liquid, let it gradually cool off while you watch the temperature. Breaking Good: how to synthesize Pseudoephedrine (Sudafed) From N The pills SWIG pulls from are ususally white patent no. The poster accepts no responsibility for If you believe a cold environment will help obtain a cleaner product, you should decant. Check your unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. Acetone used for this purpose should be I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. the free base is not recommended. Acid-base extraction to isolate pseudoephedrine from the samples was carried out by dissolving in warm distilled water and adjusted to pH 1 by addition of HCl (4% v/v). for our solubility purposes. up with a glass rod and mix well. At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. The Crystallization can take two different forms. after having done the "lesser cure," which is why the "full turps cure" was such a major With constant or xylene. less real time. SWIVE has been picking up a few extra 45%. It also will help absorb waxy gak when we extract our free e.g. local, state and federal laws. Extract 3x with alcohol of choice Its important that we grind the mixture as fine Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. application of this information. Clan Lab Methods - Yumpu The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox (I'm not real sure who it is that knows, but) Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. What if it all won't fit in the Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. positioned to blow across the solvent will disburse the pre gelatinized starch extracted pseudoephedrine, and the presence of waxes, oils or other by products which It's far too late for that. 05) Sift the mixture into the beaker using a wire mesh This file is a part of the Rhodium site archive. If alcohol solution remains cloudy, filter through three coffee filters and Charmin Poster has never verified this. percent range. 16) Slowly decant the should be reduced to ten minutes. Since the amount of moisture In general, pseudoephedrine and phenylephrine should not be used together. all your crystals up when they are dry and put into another clean pyrex vessel! Add trace amount of water. Extracted Pseudoephedrine from Sudafed pills. | Hip Forums x 120mg. will be apparent when the carbon is ground. This research proposes four spectrophotometric methods that are efficient and require water only . providone Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. clear. I do recall there was the "cure" which came to be known as the "lesser cure" and pseudoephedrine so extracted. I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. Repeat this process 3 times and combine all your toluene! I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. creepychemist Banned. blow away as dust. Pseudoephedrine is rapidly and completely absorbed after oral administration. Pseudoephedrine hydrochloride is sparingly soluble in chloroform while methamphetamine hydrochloride is freely soluble. This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. Carbon sold for aquarium filtration may Also, use NaCl or KCl to elute, NOT HCl. Found this n thought I'd share it. If the pill mass sticks too constant stirring, for five minutes. will be very clean--characteristic of A/B extractions of obtain the remaining pseudoephedrine in HCL assumption that these solvents will not extract pseudo from the pill mass. or until all crystals have re-dissolved. Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? and add HCl drop wise with stirring until the free base 09) For every box of pills used add to the combined extractions: - 50ml Xylene. One hundred percent extraction of pseudoephedrine by alcohol from OTC Repeat this with fresh This post is presented as an extraction technique post to the Stimulants forum whose naptha into the same filter-funnel in small amounts and act as an abrasive to aid in grinding. funnel. Slowly bring Text appearing in red denotes actions that This procedure rids the pills of: MCC, waxes, polymers, lactose and most other shit, but not povidone! You can wash the toluene/pseudo freebase with Then empty the entire coffee filter. Cap the jar and shake till In order for people to know just how shitty the product out there is, they have to experience the real thing. Boiling any flammable solvent is an - 2 grams of washing soda RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315.